HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 259376Generated: October 25, 2026
2-Ethylhexylamine → 2-cyano-N-(2-ethylhexyl)acetamide
https://huagongshe.com/reaction/259376
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 2-Ethylhexylamine | HCID 7719 | — |
| Reactant | Ethyl cyanoacetate | HCID 7764 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 2-cyano-N-(2-ethylhexyl)acetamide | HCID 4590704 | — |
Reaction Steps
To ethylcyanoacetate (141 g., 1.25 mole) is slowly added 2-ethylhexylamine (129 g., 1.0 mole) over a period of 0.5 hours. The solution is then gradually heated to 154° C. and the ethanol formed is collected over a period of 1.75 hours. The solution is then stripped of all volatiles boiling at or below 88° C./3.0 mm to give N-(2-ethylhexyl)cyanoacetamide, 201.5 g.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US04038065 |
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| Source dataset | uspto-grants-1977_07 |
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| ORD ID | ord-f98c1453371a44e88d48735337fef260 |
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| Source note | uspto-grants-1977_07 |
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