HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → Pentaerythritol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Trimethylolpropane | HCID 6510 | — |
| Reactant | Caprolactam | HCID 7768 | — |
| Product | Pentaerythritol | HCID 8285 | — |
Reaction Steps
Similar viscosities are obtained by initially heating the polyalcohols (a) to (d) with polyphosphoric acid (= phosphoric acid dehydrated above 200° C.), resulting once again in the formation of acid semi-esters and diester mixtures through cleavage of the anhydridic phosphorus-oxygen-phosphorus bond. These acid semi-ester and di-ester mixtures are mixed with the multicomponent mixture of 1 mol of ε-caprolactam, 1 mol of trimethylol propane and 1 mol of water.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04038198 |
| Source dataset | uspto-grants-1977_07 |
| ORD ID | ord-7ffae5f350c24d3f972a7eb9dddf251d |
| Source note | uspto-grants-1977_07 |