HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethyldithiocarbamic acid, dimethylamine → 2-Chloro-5-nitro-alpha-(nitromethyl)benzyl dimethyldithiocarbamate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethyldithiocarbamic acid, dimethylamine | HCID 11728 | — |
| Reactant | 15851-93-1 | HCID 53756732 | — |
| Solvent | Carbon Disulfide | HCID 6348 | — |
| Product | 2-Chloro-5-nitro-alpha-(nitromethyl)benzyl dimethyldithiocarbamate | HCID 21324588 | — |
Reaction Steps
As in Example 17, reaction of 2-chloro-β,5-dinitrostyrene with dimethylammonium dimethyldithiocarbamate in the presence of carbon disulfide gave 2-chloro-5-nitro-α-(nitromethyl)benzyl dimethyldithiocarbamate melting at 120° - 121° C. after recrystallization without heating from acetone-methanol solution.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04038288 |
| Source dataset | uspto-grants-1977_07 |
| ORD ID | ord-24c396fa568444ea9696d6a710ac0d10 |
| Source note | uspto-grants-1977_07 |