HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethyldithiocarbamic acid, dimethylamine → HCID 21324611, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethyldithiocarbamic acid, dimethylamine | HCID 11728 | — |
| Reactant | o-Chloro-beta-nitrostyrene | HCID 98458 | — |
| Solvent | Carbon Disulfide | HCID 6348 | — |
| Product | HCID 21324611 | HCID 21324611 | — |
Reaction Steps
As in Example 17, reaction of o-chloro-β-nitrostyrene with dimethylammonium dimethyldithiocarbamate in the presence of carbon disulfide gave o-chloro-α-(nitromethyl)benzyl dimethyldithiocarbamate melting at 102° - 103.5° C. when recrystallized without heating from acetone-methanol solution.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04038288 |
| Source dataset | uspto-grants-1977_07 |
| ORD ID | ord-6ca89d0e22a948f78e12e75d07a4d739 |
| Source note | uspto-grants-1977_07 |