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HRID259466

反应详情

EQUATION

反应方程式

HRID 259466 的结构方程式

REACTANTS

反应物

2
结构：CN(C)C(=S)[S-].C[NH2+]C
HCID11728

Dimethyldithiocarbamic acid, dimethylamine

C5H14N2S2

结构：O=[N+]([O-])C=Cc1ccc(Br)cc1
HCID274841

未命名化合物

PRODUCTS

生成物

1
结构：CN(C)C(=S)SC(C[N+](=O)[O-])c1ccc(Br)cc1
HCID21324615

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：S=C=S
溶剂HCID6348

Carbon disulfide

CS2

PROCEDURE

实验过程

As in Example 17, reaction of p-bromo-β-nitrostyrene with dimethylammonium dimethyldithiocarbamate in the presence of carbon disulfide gave p-bromo-α-(nitromethyl)benzyl dimethyldithiocarbamate melting at 79° - 81° C. when recrystallized without heating from acetone-ethanol solution.