HCID 178480602, compound → HCID 178480604, compound

HRID 259519Notes

Reaction equation

HRID 259519 reaction equation
Br[CH2:2][C:3]1[C:12]([CH2:13][OH:14])=[N+:11]([O-:15])[C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[N+:4]=1[O-:16].[SH:17][C:18]1[N:19]([CH3:23])[CH:20]=[CH:21][N:22]=1>C(Cl)(Cl)Cl>[CH3:23][N:19]1[CH:20]=[CH:21][N:22]=[C:18]1[S:17][CH2:2][C:3]1[C:12]([CH2:13][OH:14])=[N+:11]([O-:15])[C:10]2[C:5]([N+:4]=1[O-:16])=[CH:6][CH:7]=[CH:8][CH:9]=2

Participants

4

Reactant 2

HCID 178480602HCID 178480602, compoundHCID 178526280HCID 178526280, compound

Product 1

HCID 178480604HCID 178480604, compound

Reagents, catalysts & solvents 1

HCID 6212ChloroformSolvent

Procedure

2-Bromomethyl-3-hydroxymethylquinoxaline-1,4-dioxide (0.01 mole) was suspended in 75 ml of chloroform and 2-mercapto-1-methylimidazole (0.01 mole) was added in one portion. The suspension was stirred at room temperature for about 2 hours. The product was collected by filtration. Yield, 3.82 grams (96%); m.p. 174-7° ).

Workup

  1. filtrationThe product was collected by filtration
  2. customYield

Sources & evidence

ORD record
ord-f3ee9b5c99ed4885a43e6f026b468f15
Source dataset
uspto-grants-1977_07
Patent number
US04038392

Reaction notes

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