HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl trifluoroacetate → HCID 20322686, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl trifluoroacetate | HCID 9794 | — |
| Reactant | Hydrazine hydrate (1:1) | HCID 24654 | — |
| Reactant | HCID 13664048 | HCID 13664048 | — |
| Solvent | Water ethanol | HCID 19096565 | — |
| Product | HCID 20322686 | HCID 20322686 | 50% |
Reaction Steps
Prepared from ethyl-N-(4-chlorophenyl)formimidate, ethyl trifluoroacetate and hydrazine hydrate using the method of Example 1, in 50% yield m.p. 108° (from ethanol/water). (Found: C, 44.03%; H, 2.11%; Cl, 14.00%; F, 23.2%; N, 16.82%. C9H5ClF3N3 requires C, 43.66%; H, 2.04%; Cl, 14.32%; F, 23.0%; N 16.97%) δ(CDCl3): 8.37 (1H, s); 7.50 (4H, m). m/e, 247 and 249.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04038405 |
| Source dataset | uspto-grants-1977_07 |
| ORD ID | ord-b83c7e8e27ff4d778964bc10a3363f7f |
| Source note | uspto-grants-1977_07 |