HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetone → 2-(2-Methylsulfinylphenyl)oxazolo[4,5-b]pyridine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetone | HCID 180 | — |
| Reactant | 2-(2-(Methylthio)phenyl)oxazolo[4,5-b]pyridine | HCID 12461383 | — |
| Reactant | Sodium periodate | HCID 23667635 | — |
| Solvent | Water | HCID 962 | — |
| Product | 2-(2-Methylsulfinylphenyl)oxazolo[4,5-b]pyridine | HCID 22754774 | — |
Reaction Steps
A solution of 0.5 g. of 2-(2-methylthiophenyl)oxazolo[4,5-b]pyridine in 50 ml. of acetone was treated with 3 g. of sodium metaperiodate. After stirring over the weekend at room temperature, the mixture was diluted with 30 ml. of water. The acetone was distilled out and the resulting precipitate was recrystallized to give 2-(2-methylsulfinylphenyl)oxazolo[4,5-b]pyridine, m.p. 153.5°-155.5° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04038396 |
| Source dataset | uspto-grants-1977_07 |
| ORD ID | ord-8b39d698b5f24b498428dfcb1cab2f3a |
| Source note | uspto-grants-1977_07 |