HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 22402938, compound → HCID 54173576, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 22402938 | HCID 22402938 | — |
| Solvent | Acetic Anhydride | HCID 7918 | — |
| Product | HCID 54173576 | HCID 54173576 | 89.9% |
Reaction Steps
A mixture of 1,2-dimethyl-4,5-benzimidazoledicarboxylic acid (1.00 g, 4.27 mmol) and acetic anhydride (10 mL) is stirred 4 hours at reflux temperature, allowed to stand overnight at room temperature and filtered to afford the title product as yellow crystals (0.830 g, 89.8%), mp 295° C. (dec).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05523279 |
| Source dataset | uspto-grants-1996_06 |
| ORD ID | ord-cc558ee6ecc8433c946e98985e897438 |
| Source note | uspto-grants-1996_06 |