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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 259708Generated: October 28, 2026

HCID 22402938, compound → HCID 54173576, compound

https://huagongshe.com/reaction/259708

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 22402938HCID 22402938—
SolventAcetic AnhydrideHCID 7918—
ProductHCID 54173576HCID 5417357689.9%

Reaction Steps

A mixture of 1,2-dimethyl-4,5-benzimidazoledicarboxylic acid (1.00 g, 4.27 mmol) and acetic anhydride (10 mL) is stirred 4 hours at reflux temperature, allowed to stand overnight at room temperature and filtered to afford the title product as yellow crystals (0.830 g, 89.8%), mp 295° C. (dec).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05523279
Source datasetuspto-grants-1996_06
ORD IDord-cc558ee6ecc8433c946e98985e897438
Source noteuspto-grants-1996_06