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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 259713Generated: October 28, 2026

Acetic Anhydride → HCID 53661794, compound

https://huagongshe.com/reaction/259713

Reaction equation

Participants

RoleNameHCIDCharge
ReactantAcetic AnhydrideHCID 7918—
ReactantHCID 22402967HCID 22402967—
ProductHCID 53661794HCID 5366179491.1%

Reaction Conditions

Temperature0 °C

Reaction Steps

A mixture of the 1-benzyl-2-methyl-4,5-benzimidazoledicarboxylic acid (4.40 g, 14.2 mmol) and acetic anhydride is stirred for 5 hours at reflux temperature, cooled to 0° C. and filtered to give the title product as a pale yellow solid (3.78 g, 91.1%), identified by 1HNMR spectrography.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05523279
Source datasetuspto-grants-1996_06
ORD IDord-4bd3bf070b104cb297d9c6a05dbaba45
Source noteuspto-grants-1996_06