HRID25972

反应详情

EQUATION

反应方程式

HRID 25972 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

14.4 parts of isobutyraldehyde was added to 36.6 parts of benzhydrylamine in 100 parts of dry benzene at room temperature with stirring. The cloudy mixture was heated to reflux with water-separation for 4 hours. On cooling the solution was filtered to remove a small amount of solid and evaporated to give isobutylidenebenzhydrylamine.

WORKUP

后处理

  1. temperatureThe cloudy mixture was heated
  2. temperatureOn cooling the solution
  3. filtrationwas filtered
  4. customto remove a small amount of solid
  5. customevaporated