HCID 13154139, compound → HCID 22403075, compound
Reaction equation
[CH3:1][O:2][C:3]1[C:8]([O:9][CH3:10])=[CH:7][CH:6]=[CH:5][C:4]=1[C:11]1[NH:12][CH:13]=[CH:14][CH:15]=1.C(S(C1[CH:22]=[CH:23][C:24](OC)=[C:25]([C:27]2[NH:28][CH:29]=CC=2)C=1)(=O)=O)C>>[CH3:1][O:2][C:3]1[C:8]([O:9][CH3:10])=[CH:7][CH:6]=[CH:5][C:4]=1[C:11]1[NH:12][C:13]([CH2:29][N:28]2[CH2:27][CH2:25][CH2:24][CH2:23][CH2:22]2)=[CH:14][CH:15]=1Participants
3
Procedure
This compound was prepared by a method analogous to that used to prepare example 2, but using 2-(2,3-dimethoxyphenyl)-1H-pyrrole (prepared according to the method of Kruse et al., [Heterocycles, 26, 3141, 1987] from the corresponding acid chloride) in place of 2-(5-ethylsulphonyl-2-methoxyphenyl)-1H-pyrrole.
Workup
- customThis compound was prepared by a method analogous to
- customto prepare example 2
- customprepared
Sources & evidence
- ORD record
- ord-c03593551de041498efb7c4f2a697ece
- Source dataset
- uspto-grants-1996_06
- Patent number
- US05523299
Reaction notes
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