HuagongsheHuagongshe Chemistry Print Report · For research reference only
Vanillin → HCID 10563679, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Vanillin | HCID 1183 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | tert-Butyl bromoacetate | HCID 79177 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 10563679 | HCID 10563679 | — |
Reaction Steps
Vanillin was alkylated with t-butyl bromoacetate in DMF in the presence of potassium carbonate the usual way to give a waxy solid. (quant.) mp 86.8°-90° C. MS(NH3): 284 (base, M+NH4).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05523302 |
| Source dataset | uspto-grants-1996_06 |
| ORD ID | ord-6e6a95bad7f6441caac2fd5de1cce4cc |
| Source note | uspto-grants-1996_06 |