HuagongsheHuagongshe Chemistry Print Report · For research reference only
Saccharin → 1,2,3,4-Tetrahydroquinoline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Saccharin | HCID 5143 | — |
| Reactant | Iron (III) acetylacetonate | HCID 11110968 | — |
| Catalyst | Cobaltous 2-naphthenic acid | HCID 14048876 | — |
| Solvent | 3-Hydroxypropyl methacrylate | HCID 17694 | — |
| Product | 1,2,3,4-Tetrahydroquinoline | HCID 69460 | — |
Reaction Steps
An adhesive formulation prepared and tested as in Example 1 containing hydroxypropyl methacrylate (8.15 g), saccharin (0.5 g), 0.1% cobalt naphthenate in hydroxypropyl methacrylate (1 g), 0.1% iron (III) acetylacetonate in hydroxypropyl methacrylate (0.25 g) and 1,2,3,4 tetrahydroquinoline (0.5 g) gave bond strengths of 3.3 N/mm2 after 24 hours following air activation for 5 minutes.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05523347 |
| Source dataset | uspto-grants-1996_06 |
| ORD ID | ord-fd1017a35d074823bb58e407d7e7711c |
| Source note | uspto-grants-1996_06 |