HRID260101

反应详情

EQUATION

反应方程式

HRID 260101 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

84 mg of (E)-3-(3-nitro-4-methylphenyl)-2-(3,4,5-trimethoxyphenyl)-prop-2-ene-nitrile was dissolved in 8 ml of acetic acid then zinc was added to the mixture. The mixture was stirred vigorously for 1 hour then filtered and concentrated. The residue was purified on a silica gel plate (dichloromethane) to give 60 mg of the intended compound.

WORKUP

后处理

  1. filtrationthen filtered
  2. concentrationconcentrated
  3. customThe residue was purified on a silica gel plate (dichloromethane)