HRID260311

反应详情

EQUATION

反应方程式

HRID 260311 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

3

PROCEDURE

实验过程

3-Nitrocinnamic acid (1.5 g, 7.77 mM) was suspended in a mixture of ethanol (80 ml) and water (20 ml), and palladium on charcoal (10%, 100 mg) added. The mixture was shaken in an atmosphere of hydrogen for 4.5 hours, when uptake of gas complete. After filtration through diatomaceous earth, the solvent was removed to give title compound.

WORKUP

后处理

  1. additionadded
  2. filtrationAfter filtration through diatomaceous earth
  3. customthe solvent was removed