HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosphorus oxychloride → 2-(2,6-Diethyl-3-methylanilino)-2-imidazoline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosphorus oxychloride | HCID 24813 | — |
| Reactant | N-Acetylimidazolidinone | HCID 79350 | — |
| Reactant | m-Toluidine, 2,6-diethyl- | HCID 144235 | — |
| Product | 2-(2,6-Diethyl-3-methylanilino)-2-imidazoline | HCID 22401593 | — |
Reaction Steps
2,6-Diethyl-3-methyl aniline is reacted with N-acetyl-2-imidazolidinone in the presence of POCl3 to produce the imidazoline. This intermediate is treated with sodium hydroxide and water to remove the acetyl group and yield the name compound (VI).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05527830 |
| Source dataset | uspto-grants-1996_06 |
| ORD ID | ord-269305ddd5f9418ea022ac43d34bd89e |
| Source note | uspto-grants-1996_06 |