Hydrochloric Acid → HCID 22401314, compound

Participants

Reaction Steps

Using 1,2-dihydro-2-methyl-1-oxo-4-phenyl-3-isoquinoline acetic acid, diphenylphosphoryl azide and 3-(dimethylaminomethyl)aniline, the reaction was carried out by substantially the same procedure as in Method B of Example 1, followed by treatment of the product with hydrogen chloride in ethyl acetate to give the title compound as a white powdery product. NMR (200 MHz,DMSO-d6) ppm: 2.67(3H,s), 2.69(3H,s), 3.64(3H,s), 4.17(4H,m), 6.9-7.2(4H,m), 7.3-7.7(9H,m), 8.32(1H,m), 9.09(1H,bs)

Provenance & Evidence