HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Hexene → Bis(hexyldichlorosilyl)methane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Hexene | HCID 11597 | — |
| Reactant | Bisdichlorosilylmethane | HCID 57370748 | — |
| Catalyst | Chloroplatinic acid | HCID 61859 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | Bis(hexyldichlorosilyl)methane | HCID 22401807 | 72.6% |
Reaction Steps
In the same apparatus and procedures as EXAMPLE 1, 8 g(0.04 mole) of bisdichlorosilylmethane, 12.7 g (0.15 mole) of 1-hexene and 120 μl of 1% chloroplatinic acid solution in isopropanol were placed and reacted for 2 hours at reflux under the dry nitrogen atmosphere. Vacuum distillation of the reaction products gave 11.1 g (118°-120° C./0.05 mmHg) of bis(hexyldichlorosilyl)methane in 72.6% yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05527934 |
| Source dataset | uspto-grants-1996_06 |
| ORD ID | ord-32b63178f8dd4654bdf80c472de85e97 |
| Source note | uspto-grants-1996_06 |