HRID260562

反应详情

EQUATION

反应方程式

HRID 260562 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

Example 1 was repeated at 140° C. with 14.1 g of a powdered zirconium dioxide from the Aldrich company. After 2 h reaction time, the phenol conversion was 6.3%, whereby 3.2 g phenyl chloroformate and 7.8 g diphenyl carbonate were formed. The selectivity to carbonate esters was greater than 99%.

WORKUP

后处理

  1. customAfter 2 h reaction time