4-Bromobutyronitrile → HCID 22401910, compound

HRID 260603Notes

Reaction equation

HRID 260603 reaction equation
[Cl:1][C:2]1[CH:3]=[C:4]([CH:16]=[CH:17][C:18]=1[Cl:19])[CH2:5][NH:6][CH2:7][C:8]1[CH:13]=[CH:12][C:11]([Cl:14])=[C:10]([Cl:15])[CH:9]=1.Br[CH2:21][CH2:22][CH2:23][C:24]#[N:25]>>[Cl:1][C:2]1[CH:3]=[C:4]([CH:16]=[CH:17][C:18]=1[Cl:19])[CH2:5][N:6]([CH2:21][CH2:22][CH2:23][C:24]#[N:25])[CH2:7][C:8]1[CH:13]=[CH:12][C:11]([Cl:14])=[C:10]([Cl:15])[CH:9]=1

Participants

3

Reactant 2

HCID 214124-BromobutyronitrileHCID 4850930HCID 4850930, compound

Product 1

HCID 22401910HCID 22401910, compound

Procedure

Using a procedure analogous to Example 6, Bis-(3,4-dichlorobenzyl)amine (2.71 g, 8.09 mM) was reacted with 4-bromobutyronitrile (0.81 ml) to give the title compound as an oil 1.97 g.

Sources & evidence

ORD record
ord-18d66573552445e3ac64276ee855df9b
Source dataset
uspto-grants-1996_06
Patent number
US05527955

Reaction notes

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