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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 260644Generated: October 25, 2026

Chlorotrimethylsilane → 2-Benzyl-2-trimethylsilyl-1,3-dithiane

https://huagongshe.com/reaction/260644

Reaction equation

Participants

RoleNameHCIDCharge
ReactantChlorotrimethylsilaneHCID 6397—
Reactant2-Benzyl-1,3-dithianeHCID 300291—
Product2-Benzyl-2-trimethylsilyl-1,3-dithianeHCID 1046900875%

Reaction Steps

The title compound of this step was prepared in 75% yield, by the procedure described in JACS 89, (1967), 4347 by E. J. Corey, et al., using 2-benzyl-1,3-dithiane and trimethylsilyl chloride. The product was recrystallized from diethyl ether/pentane.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05529988
Source datasetuspto-grants-1996_06
ORD IDord-157274fec4e5454391c7c93903080036
Source noteuspto-grants-1996_06