HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → Nonyl indole-3-carboxylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 1-Bromononane | HCID 12742 | — |
| Reactant | Indole-3-Carboxylic Acid | HCID 69867 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | Nonyl indole-3-carboxylate | HCID 22400454 | — |
Reaction Steps
A mixture of indole-3-carboxylic acid, 1-bromononane and potassium carbonate in N,N-dimethylformamide was stirred at room temperature for 15 hours. After insoluble materials were filtered off, the filtrate was diluted with ethyl acetate, washed with water and brine, dried over magnesium sulfate and concentrated. The solid was collected and washed with hexane to give nonyl indole-3-carboxylate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05530019 |
| Source dataset | uspto-grants-1996_06 |
| ORD ID | ord-a8b8a3adb2e747c7ba5353b6483eacc7 |
| Source note | uspto-grants-1996_06 |