Ethyl 4-(3-dodecanoyl-1-indolyl)butyrate → 4-(3-Dodecanoyl-1-indolyl)butyric acid
Reaction equation
[C:1]([C:14]1[C:22]2[C:17](=[CH:18][CH:19]=[CH:20][CH:21]=2)[N:16]([CH2:23][CH2:24][CH2:25][C:26]([O:28]CC)=[O:27])[CH:15]=1)(=[O:13])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12].C(C1C2C(=CC=CC=2)N(CCCC(OCC)=O)C=1)(=O)CCCCCC>>[C:1]([C:14]1[C:22]2[C:17](=[CH:18][CH:19]=[CH:20][CH:21]=2)[N:16]([CH2:23][CH2:24][CH2:25][C:26]([OH:28])=[O:27])[CH:15]=1)(=[O:13])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12]Participants
3
Procedure
The procedure of Ex. 2 was repeated except that ethyl 4-(3-dodecanoyl-1-indolyl)butyrate obtained in Ex. 11 was used in place of ethyl 4-(3-heptanoyl-1-indolyl)butyrate to give 4-(3-dodecanoyl-1-indolyl)butyric acid.
Workup
- customobtained in Ex
Sources & evidence
- ORD record
- ord-7efa840514304ae68194248b5a49662b
- Source dataset
- uspto-grants-1996_06
- Patent number
- US05530019
Reaction notes
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