Ethyl 4-(3-tridecanoyl-1-indolyl)butyrate → 4-(3-Tridecanoyl-1-indolyl)butyric acid

HRID 260839Notes

Reaction equation

HRID 260839 reaction equation
[C:1]([C:15]1[C:23]2[C:18](=[CH:19][CH:20]=[CH:21][CH:22]=2)[N:17]([CH2:24][CH2:25][CH2:26][C:27]([O:29]CC)=[O:28])[CH:16]=1)(=[O:14])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH3:13].C(C1C2C(=CC=CC=2)N(CCCC(OCC)=O)C=1)(=O)CCCCCC>>[C:1]([C:15]1[C:23]2[C:18](=[CH:19][CH:20]=[CH:21][CH:22]=2)[N:17]([CH2:24][CH2:25][CH2:26][C:27]([OH:29])=[O:28])[CH:16]=1)(=[O:14])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH3:13]

Participants

3

Reactant 2

HCID 22400496Ethyl 4-(3-tridecanoyl-1-indolyl)butyrateHCID 22400553Ethyl 4-(3-heptanoyl-1-indolyl)butyrate

Product 1

HCID 224004934-(3-Tridecanoyl-1-indolyl)butyric acid

Procedure

The procedure of Ex. 2 was repeated except that ethyl 4-(3-tridecanoyl-1-indolyl)butyrate obtained in Ex. 13 was used in place of ethyl 4-(3-heptanoyl-1-indolyl)butyrate to give 4-(3-tridecanoyl-1-indolyl)butyric acid.

Workup

  1. customobtained in Ex

Sources & evidence

ORD record
ord-c539e4259bfd4ccdaf11015f4be7bea6
Source dataset
uspto-grants-1996_06
Patent number
US05530019

Reaction notes

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