HCID 22400515, compound → HCID 22400520, compound

HRID 260854Notes

Reaction equation

HRID 260854 reaction equation
C([O:3][C:4]([CH2:6][CH2:7][C:8]([C:10]1[C:18]2[C:13](=[CH:14][CH:15]=[CH:16][CH:17]=2)[N:12]([CH2:19][CH2:20][CH2:21][C:22]([O:24]CC)=[O:23])[CH:11]=1)=[O:9])=[O:5])C.C(C1C=CC(C(CCC)CCCCCCC(C2C3C(=CC=CC=3)N(CCCC([O-])=O)C=2)=O)=CC=1)C(C)C>>[C:4]([CH2:6][CH2:7][C:8]([C:10]1[C:18]2[C:13](=[CH:14][CH:15]=[CH:16][CH:17]=2)[N:12]([CH2:19][CH2:20][CH2:21][C:22]([OH:24])=[O:23])[CH:11]=1)=[O:9])([OH:5])=[O:3]

Participants

3

Reactant 2

HCID 22400515HCID 22400515, compoundHCID 22400538HCID 22400538, compound

Product 1

HCID 22400520HCID 22400520, compound

Procedure

The procedure of Ex. 16 was repeated except that ethyl 4-[3-(3-ethoxycarbonylpropionyl)-1-indolyl]butyrate obtained in Ex. 40 was used in place of 4-[3-[8-(4-isobutylphenyl)undecanoyl]-1-indolyl]butyrate to give 4-[3-(3-carboxy-propionyl)-1-indolyl]butyric acid as a powder.

Workup

  1. customobtained in Ex

Sources & evidence

ORD record
ord-0d5d61626d574fb8860f31f104b699a7
Source dataset
uspto-grants-1996_06
Patent number
US05530019

Reaction notes

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