HuagongsheHuagongshe Chemistry Print Report · For research reference only
Formamide, N-1-naphthalenyl- → 1-{N-[2-(1-Azabicyclo[3.3.0]octan-5-yl)ethyl]-N-formylamino}naphthalene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Formamide, N-1-naphthalenyl- | HCID 96004 | — |
| Reactant | 5-(2-Chloroethyl)-1-azabicyclo[3.3.0]octane | HCID 10702365 | — |
| Product | 1-{N-[2-(1-Azabicyclo[3.3.0]octan-5-yl)ethyl]-N-formylamino}naphthalene | HCID 10781138 | — |
Reaction Steps
The procedures described in Example 2 were repeated except that N-formyl-1-naphthylamine (1.90 g, 11.1 mmol ) and 5-(2-chloroethyl)-1-azabicyclo[3.3.0]octane (hydrochloride, 2.57 g, 12.2 mmol ) were employed In this case, the desired compound was obtained as a colorless liquid (1.80 g, 52.6%)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05530138 |
| Source dataset | uspto-grants-1996_06 |
| ORD ID | ord-246eb5d1fb184c0682be54ddb7af4258 |
| Source note | uspto-grants-1996_06 |