HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isopropylamine → Solvent Red 169
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isopropylamine | HCID 6363 | — |
| Reactant | 1-Nitroanthraquinone | HCID 6704 | — |
| Solvent | Cyclohexane | HCID 8078 | — |
| Product | Solvent Red 169 | HCID 33790 | 93.5% |
Reaction Steps
63.3 g of 1-nitroanthraquinone (99% pure) in 320 ml of cyclohexane are reacted with 147.8 g of isopropylamine (molar ratio 10:1) for 70 minutes at a temperature of 160° C. and under a pressure of 50 bars. Working up analogously to Example 1 gives 62 g (94.5% of theory) of 97.6% pure 1-isopropylamino-anthraquinone.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04163747 |
| Source dataset | uspto-grants-1979_08 |
| ORD ID | ord-203220de2fcb4ab7a612f9f8f0de48ca |
| Source note | uspto-grants-1979_08 |