Bromine → HCID 13064247, compound

HRID 261045Notes

Reaction equation

HRID 261045 reaction equation
[Cl:1][C:2]1[CH:3]=[CH:4][C:5]([OH:28])=[C:6]([CH:27]=1)[CH2:7][C:8]1[CH:13]=[C:12]([F:14])[CH:11]=[C:10]([CH:15]([C:17]2[CH:22]=[C:21]([Cl:23])[CH:20]=[C:19]([Cl:24])[C:18]=2[OH:25])[CH3:16])[C:9]=1[OH:26].[Br:29]Br>C(O)(=O)C>[Br:29][C:4]1[C:5]([OH:28])=[C:6]([CH:27]=[C:2]([Cl:1])[CH:3]=1)[CH2:7][C:8]1[CH:13]=[C:12]([F:14])[CH:11]=[C:10]([CH:15]([C:17]2[CH:22]=[C:21]([Cl:23])[CH:20]=[C:19]([Cl:24])[C:18]=2[OH:25])[CH3:16])[C:9]=1[OH:26]

Participants

4

Reactant 2

HCID 24408BromineHCID 13064250HCID 13064250, compound

Product 1

HCID 13064247HCID 13064247, compound

Reagents, catalysts & solvents 1

HCID 176Acetic AcidSolvent

Procedure

2-(5-Chloro-2-hydroxybenzyl)-6-[1-(3,5-dichloro-2-hydroxyphenyl) ethyl]-4-fluorophenol was brominated using bromine in acetic acid at room temperature to give the title compound; m.p. 171°.

Workup

  1. customat room temperature

Sources & evidence

ORD record
ord-a0eea2d9b9434e33a0f61aaf592e1c24
Source dataset
uspto-grants-1979_08
Patent number
US04163801

Reaction notes

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