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HRID261075

反应详情

EQUATION

反应方程式

HRID 261075 的结构方程式

REACTANTS

反应物

2
结构：CNC
HCID674

Dimethylamine

C2H7N

结构：CSC(=C(C#N)C#N)N(C)N=Cc1ccccc1
HCID54443969

未命名化合物

PRODUCTS

生成物

1
结构：CN(C)C(=C(C#N)C#N)N(C)N=Cc1ccccc1
HCID53665727

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCO
溶剂HCID702

Ethanol

C2H6O

CONDITIONS

反应条件

温度
0 °C

PROCEDURE

实验过程

The product of stage (a) (26 g), aqueous dimethylamine (6.6 g) and ethanol (250 ml) were heated under reflux for 4 hours and then cooled to 0° C. Benzaldehyde N-methyl-N-[2,2-dicyano-1-(dimethylamino)ethenyl]hydrazone (19.8 g) precipitated, m.p. 127°-128° C.

WORKUP

后处理

  1. temperatureunder reflux for 4 hours
  2. customBenzaldehyde N-methyl-N-[2,2-dicyano-1-(dimethylamino)ethenyl]hydrazone (19.8 g) precipitated