HuagongsheHuagongshe Chemistry Print Report · For research reference only
Homophthalic acid → 3,3-dimethyl-5-oxo-2,3-dihydro-5H-thiazolo[3,2-b]isoquinoline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Homophthalic acid | HCID 66643 | — |
| Reactant | Sodium Acetate | HCID 517045 | — |
| Reactant | 2-Amino-2-methylpropane-1-thiol | HCID 521040 | — |
| Solvent | 1,2-Dichlorobenzene | HCID 7239 | — |
| Product | 3,3-dimethyl-5-oxo-2,3-dihydro-5H-thiazolo[3,2-b]isoquinoline | HCID 12593065 | — |
Reaction Steps
By following the same procedure as in Example 49 using a mixture of 240 mg. of 2-carboxymethylbenzoic acid, 300 mg. of 2-amino-2-methylpropanethiol, 164 mg. of sodium acetate, and 5 ml. of o-dichlorobenzene, 120 mg. of 3,3-dimethyl-5-oxo-2,3-dihydro-5H-thiazolo[3,2-b]isoquinoline was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04163844 |
| Source dataset | uspto-grants-1979_08 |
| ORD ID | ord-64cfce68ca0c405c91b0742af24d77f8 |
| Source note | uspto-grants-1979_08 |