HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Naphthol → 1-Naphthol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Naphthol | HCID 8663 | — |
| Reactant | Carbamic acid, N,N-dimethyl-, ethyl ester | HCID 12709 | — |
| Catalyst | Zincchloride | HCID 3007855 | — |
| Product | 1-Naphthol | HCID 7005 | 2% |
| Product | Methyl naphthyl urethane | HCID 20396153 | — |
Reaction Steps
At 150° C. and 100 mm Hg, 14 g of beta-naphthol and 9 g of dimethyl urethane were reacted in the presence of 0.7 g ZnCl2. A conversion of 2% of naphthol to methyl naphthyl urethane was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04163861 |
| Source dataset | uspto-grants-1979_08 |
| ORD ID | ord-9f99136dc46440b0973bdac4269e2390 |
| Source note | uspto-grants-1979_08 |