Ammonia → HCID 57215693, compound

HRID 261283Notes

Reaction equation

HRID 261283 reaction equation
[N+:1]([C:4]1[C:9]([Cl:10])=[C:8]([N+:11]([O-:13])=[O:12])[CH:7]=[C:6]([CH3:14])[C:5]=1[C:15](Cl)=[O:16])([O-:3])=[O:2].[NH3:18].O>CC(C)=O>[N+:1]([C:4]1[C:9]([Cl:10])=[C:8]([N+:11]([O-:13])=[O:12])[CH:7]=[C:6]([CH3:14])[C:5]=1[C:15]([NH2:18])=[O:16])([O-:3])=[O:2]

Participants

5

Reactant 3

HCID 222AmmoniaHCID 962WaterHCID 57276841HCID 57276841, compound

Product 1

HCID 57215693HCID 57215693, compound

Reagents, catalysts & solvents 1

HCID 180AcetoneSolvent

Procedure

3,5-Dinitro-4-chloro-o-toluoyl chloride is treated with two equivalents of ammonia in cold acetone. The mixture is poured into water and the desired product as a precipitated solid collected by filtration.

Workup

  1. filtrationthe desired product as a precipitated solid collected by filtration

Sources & evidence

ORD record
ord-0f1d745fea7e47e1b3576ba60454ec12
Source dataset
uspto-grants-1979_08
Patent number
US04165231

Reaction notes

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