HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethyl Ether → N-(3-nitrophenyl)acrylamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | 3-Nitroaniline | HCID 7423 | — |
| Reactant | Acryloyl chloride | HCID 13140 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Solvent | Water | HCID 962 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | N-(3-nitrophenyl)acrylamide | HCID 12531248 | — |
Reaction Steps
To a solution of 13.8 g. (0.10 mol) of m-nitroaniline in 100 ml. of diethyl ether and 30 ml. of ethyl acetate was added 9.0 g. (0.10 mol) of acryloyl chloride and a solution of 4.0 g. (0.10 mol) of sodium hydroxide in 20 ml. of water. The mixture was stirred overnight (18 hours) at ambient temperature and the precipitate filtered to give N-propenoyl-3-nitroaniline.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04165365 |
| Source dataset | uspto-grants-1979_08 |
| ORD ID | ord-835773b9069f4a10aaac51a392a71f7f |
| Source note | uspto-grants-1979_08 |