反应详情

A mixture of 0.915 g (3.3 mmole) of N-(3-amino-5-nitrophenyl)-2,2-dimethyl-1,3-dioxolane-4-carboxamide in 20 ml of 50% acetic acid was heated on a steam bath for 1 hour then stored over a weekend. The solvents were removed in high vacuum to afford the product, N-(2,3-dihydroxypropionyl)-3-amino-5-nitroaniline, as an oil which was used without further purification.

1. temperaturewas heated on a steam bath for 1 hour
2. waitthen stored over a weekend
3. customThe solvents were removed in high vacuum