HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Mercaptoethanol → 2-(6-Carboxyhexyl)-4-(2-hydroxyethylthio)cyclopent-2-en-1-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Mercaptoethanol | HCID 1567 | — |
| Reactant | ACMC-20apjz | HCID 3690897 | — |
| Reactant | Sodium Methoxide | HCID 10942334 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 2-(6-Carboxyhexyl)-4-(2-hydroxyethylthio)cyclopent-2-en-1-one | HCID 23346654 | — |
Reaction Steps
In the manner of Example 281 a methanol solution of 2-(6-carboxyhexyl)-4-hydroxycyclopent-2-en-1-one [Prostaglandins, 3, 921 (1973)] and β-mercaptoethanol is treated with sodium methoxide solution, acidified, concentrated, and extracted to provide the subject compound as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04165331 |
| Source dataset | uspto-grants-1979_08 |
| ORD ID | ord-30160fcc15e5467ca5ce4ce942634e16 |
| Source note | uspto-grants-1979_08 |