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HRID26144

反应详情

EQUATION

反应方程式

HRID 26144 的结构方程式

REACTANTS

反应物

2
结构：CN(C)C(=S)[S-].C[NH2+]C
HCID11728

Dimethyldithiocarbamic acid, dimethylamine

C5H14N2S2

结构：O=[N+]([O-])C=Cc1cc([N+](=O)[O-])ccc1Cl
HCID53756732

未命名化合物

PRODUCTS

生成物

1
结构：CN(C)C(=S)SC(C[N+](=O)[O-])c1cc([N+](=O)[O-])ccc1Cl
HCID21324588

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：S=C=S
溶剂HCID6348

Carbon disulfide

CS2

PROCEDURE

实验过程

As in Example 17, reaction of 2-chloro-β,5-dinitrostyrene with dimethylammonium dimethyldithiocarbamate in the presence of carbon disulfide gave 2-chloro-5-nitro-α-(nitromethyl)benzyl dimethyldithiocarbamate melting at 120° C.-121° C. after recrystallization without heating from acetone-methanol solution.