huagongshe.com
HRID26146

反应详情

EQUATION

反应方程式

HRID 26146 的结构方程式

REACTANTS

反应物

2
结构：CN(C)C(=S)[S-].C[NH2+]C
HCID11728

Dimethyldithiocarbamic acid, dimethylamine

C5H14N2S2

结构：COc1ccc(C=C[N+](=O)[O-])cc1OC
HCID222093

未命名化合物

PRODUCTS

生成物

1
结构：COc1ccc(C(C[N+](=O)[O-])SC(=S)N(C)C)cc1OC
HCID21324596

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：S=C=S
溶剂HCID6348

Carbon disulfide

CS2

PROCEDURE

实验过程

As in Example 17, reaction of 3,4-dimethoxy-β-nitrostyrene with dimethylammonium dimethyldithiocarbamate in the presence of carbon disulfide gave 3,4-dimethoxy-α-(nitromethyl)-benzyl dimethyldithiocarbamate melting at 108° C.-110° C. after recrystallization without heating from acetone-methanol solution.