HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethyldithiocarbamic acid, dimethylamine → p-Isopropyl-alpha-(nitromethyl)benzyl dimethyldithiocarbamate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethyldithiocarbamic acid, dimethylamine | HCID 11728 | — |
| Reactant | p-Isopropyl-beta-nitrostyrene | HCID 2737867 | — |
| Solvent | Carbon Disulfide | HCID 6348 | — |
| Product | p-Isopropyl-alpha-(nitromethyl)benzyl dimethyldithiocarbamate | HCID 21324607 | — |
Reaction Steps
As in Example 17, reaction of p-isopropyl-β-nitrostyrene with dimethylammonium dimethyldithiocarbamate in the presence of carbon disulfide gave p-isopropyl-α-(nitromethyl)benzyl dimethyldithiocarbamate melting at 119° C.-120° C. after recrystallization without heating from acetone-methanol solution.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04148795 |
| Source dataset | uspto-grants-1979_04 |
| ORD ID | ord-833805dd93264c1d9fd2dab4a47433ab |
| Source note | uspto-grants-1979_04 |