HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,4-Dichloroaniline → HCID 19006421, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,4-Dichloroaniline | HCID 7257 | — |
| Reactant | HCID 178504154 | HCID 178504154 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 19006421 | HCID 19006421 | — |
Reaction Steps
3.0 g of N-(2,6-dichlorothiobenzoyl)-S-methyldithiocarbamate and 1.6 g of 3,4-dichloroaniline are dissolved in 25 ml of toluene and subsequently heated while refluxing for 5 hours. The resulting yellow precipitate is worked up in the usual manner. Yield 2.1 g. Melting point 168°-170° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04166124 |
| Source dataset | uspto-grants-1979_08 |
| ORD ID | ord-c4a9c85ce4f74bb69a2a53be64022ae3 |
| Source note | uspto-grants-1979_08 |