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HRID26149

反应详情

EQUATION

反应方程式

HRID 26149 的结构方程式

REACTANTS

反应物

2
结构：CN(C)C(=S)[S-].C[NH2+]C
HCID11728

Dimethyldithiocarbamic acid, dimethylamine

C5H14N2S2

结构：O=[N+]([O-])C=Cc1ccc2c(c1)OCO2
HCID94945

5-(2-Nitroethenyl)-1,3-benzodioxole

C9H7NO4

PRODUCTS

生成物

1
结构：CN(C)C(=S)SC(C[N+](=O)[O-])c1ccc2c(c1)OCO2
HCID21324627

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：S=C=S
溶剂HCID6348

Carbon disulfide

CS2

PROCEDURE

实验过程

As in Example 17, reaction of 3,4-(methylenedioxy)-β-nitrostyrene with dimethylammonium dimethyldithiocarbamate in the presence of carbon disulfide gave 3,4-(methylenedioxy)-α-(nitromethyl)benzyl dimethyldithiocarbamate melting at 122° C.-124° C. when recrystallized without heating from acetone-ethanol solution.