HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethyldithiocarbamic acid, dimethylamine → HCID 21324615, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethyldithiocarbamic acid, dimethylamine | HCID 11728 | — |
| Reactant | HCID 274841 | HCID 274841 | — |
| Solvent | Carbon Disulfide | HCID 6348 | — |
| Product | HCID 21324615 | HCID 21324615 | — |
Reaction Steps
As in Example 17, reaction of p-bromo-β-nitrostyrene with dimethylammonium dimethyldithiocarbamate in the presence of carbon disulfide gave p-bromo-α-(nitromethyl)benzyl dimethyldithiocarbamate melting at 70° C.-81° C. when recrystallized without heating from acetone-ethanol solution.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04148795 |
| Source dataset | uspto-grants-1979_04 |
| ORD ID | ord-f9568d0913d747759d9f7dba71709d95 |
| Source note | uspto-grants-1979_04 |