HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethyldithiocarbamic acid, dimethylamine → alpha-(Nitromethyl)furfuryl dimethyldithiocarbamate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethyldithiocarbamic acid, dimethylamine | HCID 11728 | — |
| Reactant | Furan, 2-[(1E)-2-nitroethenyl]- | HCID 12781 | — |
| Solvent | Carbon Disulfide | HCID 6348 | — |
| Product | alpha-(Nitromethyl)furfuryl dimethyldithiocarbamate | HCID 21324594 | — |
Reaction Steps
As in Example 17, reaction of 2-(2-nitrovinyl)furan with dimethylammonium dimethyldithiocarbamate in the presence of carbon disulfide gave α-(nitromethyl)furfuryl dimethyldithiocarbamate melting at 67° C.-68° C. after recrystallization from methanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04148795 |
| Source dataset | uspto-grants-1979_04 |
| ORD ID | ord-efab35ff0bd1482aba08eab7670597e6 |
| Source note | uspto-grants-1979_04 |