Cyclohexylammonium Ion → (2-Methyl-2,3-dihydro-1H-inden-5-yl)acetic acid
Reaction equation
C[O:2][C:3](=[O:16])[C:4](=O)[C:5]1[CH:6]=[C:7]2[C:11](=[CH:12][CH:13]=1)[CH2:10][CH:9]([CH3:14])[CH2:8]2.C1([NH3+])CCCCC1>>[CH3:14][CH:9]1[CH2:8][C:7]2[C:11](=[CH:12][CH:13]=[C:5]([CH2:4][C:3]([OH:16])=[O:2])[CH:6]=2)[CH2:10]1Participants
3
Procedure
α-oxo-2-methyl-5-indanacetic acid methyl ester is reduced in a manner analogous to that described in Example 4. The cyclohexyl-ammonium salt of the title compound has a M.P. of 175°-178°.
Sources & evidence
- ORD record
- ord-8dc9bf3fa48441c2a6cded68176698c5
- Source dataset
- uspto-grants-1979_08
- Patent number
- US04166131
Reaction notes
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