3,4-Dimethoxy-beta-nitrostyrene → 3,4-Dimethoxy-alpha-(nitromethyl)benzyl ethyldithiocarbanilate

HRID 26155Notes

Reaction equation

[CH3:1][O:2][C:3]1[CH:4]=[C:5]([CH:11]=[CH:12][C:13]=1[O:14][CH3:15])[CH:6]=[CH:7][N+:8]([O-:10])=[O:9].[CH2:16]([N:18]([C:22]1[CH:27]=[CH:26][CH:25]=[CH:24][CH:23]=1)[C:19](=[S:21])[S-:20])[CH3:17].[NH4+]>>[CH2:16]([N:18]([C:22]1[CH:27]=[CH:26][CH:25]=[CH:24][CH:23]=1)[C:19](=[S:20])[S:21][CH:6]([CH2:7][N+:8]([O-:10])=[O:9])[C:5]1[CH:11]=[CH:12][C:13]([O:14][CH3:15])=[C:3]([O:2][CH3:1])[CH:4]=1)[CH3:17]

Participants

Reactant 2

HCID 2220933,4-Dimethoxy-beta-nitrostyrene

HCID 86734535Ammonium ethyldithiocarbanilate

Product 1

HCID 542908273,4-Dimethoxy-alpha-(nitromethyl)benzyl ethyldithiocarbanilate

Procedure

Reaction of 3,4-dimethoxy-β-nitrostyrene with ammonium ethyldithiocarbanilate by the above procedure yields 3,4-dimethoxy-α-(nitromethyl)benzyl ethyldithiocarbanilate.

Sources & evidence

ORD record: ord-729ef23a422b496980b5a66d5ad56d01
Source dataset: uspto-grants-1979_04
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04148795

Reaction notes

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