2,3-Dimethylphenylisothiocyanate → 2-(2,3-Dimethyl-phenylimino)-3-methyl-thiazoline
Reaction equation
C[C:2]1C=C(C)C=C[C:3]=1[N:9]=[C:10]=S.[CH3:12][C:13]1[C:18]([CH3:19])=[CH:17][CH:16]=[CH:15][C:14]=1[N:20]=[C:21]=[S:22]>>[CH3:12][C:13]1[C:18]([CH3:19])=[CH:17][CH:16]=[CH:15][C:14]=1[N:20]=[C:21]1[N:9]([CH3:10])[CH:3]=[CH:2][S:22]1Participants
3
Procedure
If 2,4-dimethyl-phenyl isothiocyanate in the above example is replaced by the same amount of 2,3-dimethyl-phenyl isothiocyanate and the procedure followed is an indicated, a solution of 2-(2,3-dimethyl-phenylimino)-3-methyl-thiazoline is obtained in a similar concentration and yield.
Sources & evidence
- ORD record
- ord-0345c5b6738648568765d07f8502eae8
- Source dataset
- uspto-grants-1979_04
- Patent number
- US04148799
Reaction notes
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