HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → 3-Amino-7-benzamidoheptan-2-one hydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 3,7-Dibenzamidoheptan-2-one | HCID 12769838 | — |
| Product | 3-Amino-7-benzamidoheptan-2-one hydrochloride | HCID 20394568 | 34.2% |
Reaction Steps
3,7-Dibenzamidoheptan-2-one (91.11 g, 0.258 mol) was hydrolysed in a sealed tube with concentrated HCl for 3 hours at 160° (oil bath). The solution was extracted with ether and evaporated to dryness to give 3-amino-7-benzamidoheptan-2-one hydrochloride (25.01 g, 34.2%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04166184 |
| Source dataset | uspto-grants-1979_08 |
| ORD ID | ord-0dfa7767110e41af95b6413b4d86f4d6 |
| Source note | uspto-grants-1979_08 |