HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chloroacetanilide → 10-Hydroxy-5,5-dimethyl-8-(1,2-dimethylheptyl)-N-phenyl-1,2,3,4-tetrahydro-5H-[1]benzopyrano[4,3-c]pyridine-2-acetamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chloroacetanilide | HCID 11485 | — |
| Reactant | 5H-(1)Benzopyrano(4,3-c)pyridine, 1,2,3,4-tetrahydro-5,5-dimethyl-8-(1,2-dimethylheptyl)-10-hydroxy- | HCID 213543 | — |
| Product | 10-Hydroxy-5,5-dimethyl-8-(1,2-dimethylheptyl)-N-phenyl-1,2,3,4-tetrahydro-5H-[1]benzopyrano[4,3-c]pyridine-2-acetamide | HCID 21321142 | — |
Reaction Steps
The above-titled compound was prepared by reacting 10-hydroxy-5,5-dimethyl-8-(1,2-dimethylheptyl)-1,2,3,4-tetrahydro-5H-[1]benzopyrano[4,3-c]pyridine with 2-chloro-N-phenylacetamide according to the method of Example 1; m.p. 125°-127°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04152327 |
| Source dataset | uspto-grants-1979_05 |
| ORD ID | ord-934dcf55f92d4aae88eadbd1a3a6580e |
| Source note | uspto-grants-1979_05 |