Dimethyl N-cyanodithioiminocarbonate → HCID 178504042, compound
Reaction equation
[NH2:1][CH2:2][CH2:3][S:4][CH2:5][C:6]1[CH:11]=[CH:10][CH:9]=[CH:8][N:7]=1.[CH3:12][S:13][C:14](=[N:17]C#N)SC>>[N:7]1[CH:8]=[CH:9][CH:10]=[CH:11][C:6]=1[CH2:5][S:4][CH2:3][CH2:2][NH:1][C:14](=[NH:17])[S:13][CH3:12]Participants
3
Procedure
The reaction of 2-((2-aminoethyl)thiomethyl)pyridine with dimethylcyanodithioimidocarbonate by a method similar to that described in Example (3d) afforded N-cyano-N'-[(2-(2-pyridylmethylthio)ethyl]-S-methylisothiourea, m.p. 85 - 88°. (from isopropyl alcohol-ether)
Sources & evidence
- ORD record
- ord-d27c548a8a9948beae40529474176c6e
- Source dataset
- uspto-grants-1979_05
- Patent number
- US04152443
Reaction notes
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