2-Pyridineethanamine → HCID 178512332, compound

HRID 261814Notes

Reaction equation

HRID 261814 reaction equation
[C:1]([NH:3][C:4](=[N:7][CH2:8][CH2:9][S:10][CH2:11][C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][N:13]=1)SC)#[N:2].NC[CH2:20][C:21]1[CH:26]=[CH:25][CH:24]=[CH:23][N:22]=1>>[N:22]1[CH:23]=[CH:24][CH:25]=[CH:26][C:21]=1[CH2:20][S:10][CH2:9][CH2:8][NH:7][C:4]([NH:7][CH2:8][CH2:9][S:10][CH2:11][C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][N:13]=1)=[N:3][C:1]#[N:2]

Participants

3

Reactant 2

HCID 759192-PyridineethanamineHCID 12889408N-cyano-N'[2-(2-pyridylmethylthio)ethyl]-S-methylisothiourea

Product 1

HCID 178512332HCID 178512332, compound

Procedure

The reaction of N-cyano-N'-[2-(2-pyridylmethylthio)ethyl]-S-methylisothiourea with 2-((2-aminoethyl)pyridine by the method described in Example 7 afforded the title compound m.p. 78°-80°.

Sources & evidence

ORD record
ord-953d606624d6457dab7bed60380d9876
Source dataset
uspto-grants-1979_05
Patent number
US04152443

Reaction notes

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